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Fast and Stable Electrochemical Production of H2O2by Electrode Architecture Engineering

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A1 Alkuperäisartikkeli tieteellisessä aikakauslehdessä

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en

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10

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ACS Sustainable Chemistry & Engineering, Volume 9, issue 20, pp. 7120-7129

Abstract

Fast and stable production of hydrogen peroxide (H2O2) through electrochemical pathways is crucial for wastewater treatment applications. With this objective, herein, we report an integrated and superaerophilic electrode composed of atomically dispersed Ni-O-C site-enriched carbon nanosheets (IS-NiOC electrode) for electrochemical oxygen reduction to produce H2O2. Both experimental and theoretical results have proven that atomically dispersed Ni-O-C sites enable a low overpotential (260 mV at 0.1 mA cm-2) and high selectivity (>90% at 0.0-0.5 V vs reversible hydrogen electrode (RHE)) in a neutral electrolyte. Compared with a commercial gas-diffusion electrode, the IS-NiOC electrode offers stronger affinity to oxygen bubbles and more robust three-phase contact points, resulting in high current density (∼106 mA cm-2 at 0.25 V vs RHE) and superior stability (∼200 h). These merits allow the application of the IS-NiOC electrode in an electro-Fenton-like process, which enables fast degradation of representative organic pollutants in both a steady state and a flow state.

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Funding Information: This work was supported by the Ningbo S&T Innovation 2025 Major Special Program (2020Z059 and 2020Z107), the BoXin project (BX20190339), the Natural Science Foundation of Ningbo (Nos. 2019A610442 and 202003N4351), the China Postdoctoral Science Foundation (Nos. 2019M662127and 2019M662124), and the Hundred Talents Programs in Chinese Academy of Science. The DFT calculation was supported by the High-Performance Computing Center of Collaborative Innovation Center of Advanced Microstructures, Nanjing University. Publisher Copyright: ©

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Xu, W, Liang, Z, Gong, S, Zhang, B, Wang, H, Su, L, Chen, X, Han, N, Tian, Z, Kallio, T, Chen, L, Lu, Z & Sun, X 2021, 'Fast and Stable Electrochemical Production of H 2 O 2 by Electrode Architecture Engineering', ACS Sustainable Chemistry & Engineering, vol. 9, no. 20, pp. 7120-7129. https://doi.org/10.1021/acssuschemeng.1c01468

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