An expedient synthesis of D-callipeltose

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Journal Title

Journal ISSN

Volume Title

A1 Alkuperäisartikkeli tieteellisessä aikakauslehdessä

Date

2001

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Mcode

Degree programme

Language

en

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Series

TETRAHEDRON-ASYMMETRY, Volume 12, pp. 937-942

Abstract

Methyl D-callipeltose 12 and D-callipeltose 4 were synthesized from D-glucal 5 in 10 and 11 steps, respectively. The synthesis features an azide displacement reaction of an -nosyloxy ketone 7 and a highly diastereoselective C-methylation of alpha-azido ketone 8.

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Keywords

azides, D-callipeltose, D-glucal, diastereoselective synthesis

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Citation

Pihko, A J, Nicolaou, K C & Koskinen, A M P 2001, ' An expedient synthesis of D-callipeltose ', TETRAHEDRON-ASYMMETRY, vol. 12, pp. 937-942 . https://doi.org/10.1016/S0957-4166(01)00146-X