Atomic layer deposited zinc promoted copper catalysts for carbon dioxide hydrogenation to methanol : Influence of support

Loading...
Thumbnail Image

Access rights

openAccess
CC BY
publishedVersion

URL

Journal Title

Journal ISSN

Volume Title

A1 Alkuperäisartikkeli tieteellisessä aikakauslehdessä

Date

2025-06-15

Major/Subject

Mcode

Degree programme

Language

en

Pages

11

Series

Catalysis Today, Volume 454

Abstract

Copper promoted with zinc is an active catalyst for carbon dioxide hydrogenation to methanol, a reaction relevant to carbon capture and utilization technologies. Previous work showed that inverse zinc-on-copper catalysts on zirconia supports, where zinc(II) is added via atomic layer deposition (ALD), are more active and selective in this reaction than copper-on-zinc catalysts on zirconia. This work continues exploring the inverse zinc-on-copper catalysts by varying the support, comparing zirconia support with alumina, titania and niobia, and with various combinations of the ceria-zirconia-lanthana mixed oxide family. Catalyst characterization was made with elemental analysis, temperature-programmed reduction, temperature-programmed desorption of carbon dioxide, nitrous oxide pulse titration, and transmission electron microscopy. Activity was measured in a fixed-bed flow reactor at 450–550 K. ALD of Zn(II) acetylacetonate gave a similar areal number density of ca. two zinc per square nanometer on all tested supports. Zinc promotion systematically increased the methanol production rate. Among the tested catalysts, the zinc-on-copper on zirconia support remained the most active, with other catalysts from the ceria-zirconia-lanthana mixed oxide family giving almost as good results.

Description

Publisher Copyright: © 2025 The Authors

Keywords

Atomic layer deposition, Carbon dioxide, Copper, Hydrogenation, Methanol, Zinc oxide

Other note

Citation

Arandia, A, Velasco, J A, Sajid, A, Yim, J, Shamshad, H, Jiang, H, Chahal, A, Singh, A K, Gonsalves, C, Karinen, R & Puurunen, R L 2025, ' Atomic layer deposited zinc promoted copper catalysts for carbon dioxide hydrogenation to methanol : Influence of support ', Catalysis Today, vol. 454, 115283 . https://doi.org/10.1016/j.cattod.2025.115283