The human factor: results of a small-angle scattering data analysis round robin

dc.contributorAalto-yliopistofi
dc.contributorAalto Universityen
dc.contributor.authorPauw, Brian R.en_US
dc.contributor.authorSmales, Glen J.en_US
dc.contributor.authorAnker, Andy S.en_US
dc.contributor.authorAnnadurai, Venkatasamyen_US
dc.contributor.authorBalazs, Daniel M.en_US
dc.contributor.authorBienert, Ralfen_US
dc.contributor.authorBouwman, Wim G.en_US
dc.contributor.authorBreßler, Ingoen_US
dc.contributor.authorBreternitz, Joachimen_US
dc.contributor.authorBrok, Erik S.en_US
dc.contributor.authorBryant, Garyen_US
dc.contributor.authorClulow, Andrew J.en_US
dc.contributor.authorCrater, Erin R.en_US
dc.contributor.authorDe Geuser, Frédéricen_US
dc.contributor.authorGiudice, Alessandra Delen_US
dc.contributor.authorDeumer, Jérômeen_US
dc.contributor.authorDisch, Sabrinaen_US
dc.contributor.authorDutt, Shankaren_US
dc.contributor.authorFrank, Kilianen_US
dc.contributor.authorFratini, Emilianoen_US
dc.contributor.authorGarcia, Paulo R.A.F.en_US
dc.contributor.authorGilbert, Elliot P.en_US
dc.contributor.authorHahn, Marc B.en_US
dc.contributor.authorHallett, Jamesen_US
dc.contributor.authorHohenschutz, Maxen_US
dc.contributor.authorHollamby, Martinen_US
dc.contributor.authorHuband, Stevenen_US
dc.contributor.authorIlavsky, Janen_US
dc.contributor.authorJochum, Johanna K.en_US
dc.contributor.authorJuelsholt, Mikkelen_US
dc.contributor.authorMansel, Bradley W.en_US
dc.contributor.authorPenttilä, Paavoen_US
dc.contributor.authorPittkowski, Rebecca K.en_US
dc.contributor.authorPortale, Giuseppeen_US
dc.contributor.authorPozzo, Lilo D.en_US
dc.contributor.authorRochels, Leonharden_US
dc.contributor.authorRosalie, Julian M.en_US
dc.contributor.authorSaloga, Patrick E.J.en_US
dc.contributor.authorSeibt, Susanneen_US
dc.contributor.authorSmith, Andrew J.en_US
dc.contributor.authorSmith, Gregory N.en_US
dc.contributor.authorSpiering, Glenn A.en_US
dc.contributor.authorStawski, Tomasz M.en_US
dc.contributor.authorTaché, Olivieren_US
dc.contributor.authorThünemann, Andreas F.en_US
dc.contributor.authorToth, Kristofen_US
dc.contributor.authorWhitten, Andrew E.en_US
dc.contributor.authorWuttke, Joachimen_US
dc.contributor.departmentDepartment of Bioproducts and Biosystemsen
dc.contributor.groupauthorWood Material Scienceen
dc.contributor.organizationFederal Institute for Materials Research and Testingen_US
dc.contributor.organizationUniversity of Copenhagenen_US
dc.contributor.organizationUniversity of Mysoreen_US
dc.contributor.organizationInstitute of Science and Technology Austriaen_US
dc.contributor.organizationDelft University of Technologyen_US
dc.contributor.organizationHelmholtz Centre Berlin for Materials and Energyen_US
dc.contributor.organizationFORCE Technologyen_US
dc.contributor.organizationRMIT Universityen_US
dc.contributor.organizationAustralian Synchrotronen_US
dc.contributor.organizationVirginia Polytechnic Institute and State Universityen_US
dc.contributor.organizationUniversité Grenoble Alpesen_US
dc.contributor.organizationSapienza University of Romeen_US
dc.contributor.organizationPhysikalisch-Technische Bundesanstalten_US
dc.contributor.organizationUniversity of Cologneen_US
dc.contributor.organizationAustralian National Universityen_US
dc.contributor.organizationLudwig Maximilian University of Munichen_US
dc.contributor.organizationUniversity of Florenceen_US
dc.contributor.organizationBrazilian Synchrotron Light Laboratoryen_US
dc.contributor.organizationAustralian Nuclear Science and Technology Organisationen_US
dc.contributor.organizationUniversity of Readingen_US
dc.contributor.organizationRWTH Aachen Universityen_US
dc.contributor.organizationKeele Universityen_US
dc.contributor.organizationUniversity of Warwicken_US
dc.contributor.organizationArgonne National Laboratoryen_US
dc.contributor.organizationTechnical University of Munichen_US
dc.contributor.organizationUniversity of Oxforden_US
dc.contributor.organizationNational Synchrotron Radiation Research Centeren_US
dc.contributor.organizationUniversity of Groningenen_US
dc.contributor.organizationUniversity of Washingtonen_US
dc.contributor.organizationIndependent Researcher, Germanyen_US
dc.contributor.organizationDiamond Light Source Ltden_US
dc.contributor.organizationRutherford Appleton Laboratoryen_US
dc.contributor.organizationUniversité Paris-Saclayen_US
dc.contributor.organizationNational Institute of Standards and Technology NISTen_US
dc.contributor.organizationForschungszentrum Jülichen_US
dc.date.accessioned2024-01-31T08:16:26Z
dc.date.available2024-01-31T08:16:26Z
dc.date.issued2023-12-01en_US
dc.descriptionFunding Information: KT acknowledges the NIST–NRC postdoctoral fellowship program for support. This work was partially funded through the European Metrology Programme for Innovation and Research (EMPIR) project No. 17NRM04. Publisher Copyright: © 2023 International Union of Crystallography. All rights reserved.
dc.description.abstractA round-robin study has been carried out to estimate the impact of the human element in small-angle scattering data analysis. Four corrected datasets were provided to participants ready for analysis. All datasets were measured on samples containing spherical scatterers, with two datasets in dilute dispersions and two from powders. Most of the 46 participants correctly identified the number of populations in the dilute dispersions, with half of the population mean entries within 1.5% and half of the population width entries within 40%. Due to the added complexity of the structure factor, far fewer people submitted answers on the powder datasets. For those that did, half of the entries for the means and widths were within 44 and 86%, respectively. This round-robin experiment highlights several causes for the discrepancies, for which solutions are proposed.en
dc.description.versionPeer revieweden
dc.format.extent12
dc.format.extent1618-1629
dc.format.mimetypeapplication/pdfen_US
dc.identifier.citationPauw, B R, Smales, G J, Anker, A S, Annadurai, V, Balazs, D M, Bienert, R, Bouwman, W G, Breßler, I, Breternitz, J, Brok, E S, Bryant, G, Clulow, A J, Crater, E R, De Geuser, F, Giudice, A D, Deumer, J, Disch, S, Dutt, S, Frank, K, Fratini, E, Garcia, P R A F, Gilbert, E P, Hahn, M B, Hallett, J, Hohenschutz, M, Hollamby, M, Huband, S, Ilavsky, J, Jochum, J K, Juelsholt, M, Mansel, B W, Penttilä, P, Pittkowski, R K, Portale, G, Pozzo, L D, Rochels, L, Rosalie, J M, Saloga, P E J, Seibt, S, Smith, A J, Smith, G N, Spiering, G A, Stawski, T M, Taché, O, Thünemann, A F, Toth, K, Whitten, A E & Wuttke, J 2023, ' The human factor: results of a small-angle scattering data analysis round robin ', Journal of Applied Crystallography, vol. 56, no. 6 Pt, pp. 1618-1629 . https://doi.org/10.1107/S1600576723008324en
dc.identifier.doi10.1107/S1600576723008324en_US
dc.identifier.issn0021-8898
dc.identifier.otherPURE UUID: 68eec5a5-0ed0-4cea-a177-375d1e982a44en_US
dc.identifier.otherPURE ITEMURL: https://research.aalto.fi/en/publications/68eec5a5-0ed0-4cea-a177-375d1e982a44en_US
dc.identifier.otherPURE LINK: http://www.scopus.com/inward/record.url?scp=85181743175&partnerID=8YFLogxKen_US
dc.identifier.otherPURE LINK: https://doi.org/10.5281/zenodo.7506365en_US
dc.identifier.otherPURE LINK: https://doi.org/10.5281/zenodo.7509710en_US
dc.identifier.otherPURE FILEURL: https://research.aalto.fi/files/134932459/CHEM_Pauw_et_al_The_human_factor_2023_J_Appl_Cryst.pdfen_US
dc.identifier.urihttps://aaltodoc.aalto.fi/handle/123456789/126549
dc.identifier.urnURN:NBN:fi:aalto-202401312216
dc.language.isoenen
dc.publisherInternational Union of Crystallography
dc.relation.ispartofseriesJournal of Applied Crystallographyen
dc.relation.ispartofseriesVolume 56, issue 6 Pten
dc.rightsopenAccessen
dc.subject.keyworddata analysisen_US
dc.subject.keywordinterlaboratory comparabilityen_US
dc.subject.keywordnanomaterialsen_US
dc.subject.keywordnanostructure quantificationen_US
dc.subject.keywordround robinsen_US
dc.subject.keywordsmall-angle scatteringen_US
dc.titleThe human factor: results of a small-angle scattering data analysis round robinen
dc.typeA1 Alkuperäisartikkeli tieteellisessä aikakauslehdessäfi
dc.type.versionpublishedVersion
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