Synchrotron radiation x-ray topography and defect selective etching analysis of threading dislocations in GaN

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© 2014 American Institute of Physics. This article may be downloaded for personal use only. Any other use requires prior permission of the author and the American Institute of Physics. http://scitation.aip.org/content/aip/journal/jap
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Volume Title

School of Electrical Engineering | A1 Alkuperäisartikkeli tieteellisessä aikakauslehdessä

Date

2014

Major/Subject

Mcode

Degree programme

Language

en

Pages

083504/1-9

Series

Journal of Applied Physics, Volume 116, Issue 8

Abstract

The crystal quality of bulk GaN crystals is continuously improving due to advances in GaN growth techniques. Defect characterization of the GaN substrates by conventional methods is impeded by the very low dislocation density and a large scale defect analysis method is needed. White beam synchrotron radiation x-ray topography (SR-XRT) is a rapid and non-destructive technique for dislocation analysis on a large scale. In this study, the defect structure of an ammonothermal c-plane GaN substrate was recorded using SR-XRT and the image contrast caused by the dislocation induced microstrain was simulated. The simulations and experimental observations agree excellently and the SR-XRT image contrasts of mixed and screw dislocations were determined. Apart from a few exceptions, defect selective etching measurements were shown to correspond one to one with the SR-XRT results.

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Keywords

dislocations, etching, x-ray diffraction, topography, epitaxy

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Citation

Sintonen, Sakari & Rudzinski, Mariusz & Suihkonen, Sami & Jussila, Henri & Knetzger, Michael & Meissner, Elke & Danilewsky, Andreas & Tuomi, Turkka O. & Lipsanen, Harri. 2014. Synchrotron radiation x-ray topography and defect selective etching analysis of threading dislocations in GaN. Journal of Applied Physics. Volume 116, Issue 8. P. 083504/1-9. ISSN 0021-8979 (printed). DOI: 10.1063/1.4893901.